Erosion of an aluminium oxide surface as well as a formation of an aluminium oxide coating on an aluminium substrate, comparable with erosion and oxide formation induced by plasma electrolytic oxidation (PEO), can be caused at atmospheric pressure conditions by a DBD-like (dielectric barrier discharge) plasma jet. Obtained experimental results conform a previously assumed similarity of the erosion mechanisms induced by the atmospheric pressure DBD-like plasma jet and PEO microdischarges. The mechanism of a predominantly inward growth of the oxide layer during PEO processing is substantiated based on a comparison of aluminium oxide erosion and oxide layer deposition by a treatment with the considered He-plasma jet and a PEO process.
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Release Date | 2023-04-11 |
Identifier | 75e1dab1-af1a-42a6-a710-12ef83376410 |
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Plasma Source Procedure | DBD-like He-plasma jet: As substrate, small plates of an aluminium alloy (AW-6061) with a dimension of 20 mm × 20 mm × 2 mm are used. The gas flow dynamics of the plasma jet effluent can be influenced by additional lateral gas flows. The substrate surface is covered with two glass plates of 1 mm thickness and with polished edges, which are pressed together to study an influence of a thin dielectric slit on the erosion of aluminium or an aluminium oxide layer.
PEO microdischarge ignitions: Distilled water with the addition of 1 g/l potassium hydroxide serves as electrolyte for both processes, the preliminary anodisation and the PEO process. |
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Plasma Medium Properties | The DBD-like He-plasma jet is operated with pure helium (Alphagaz, 5.0), which is transported with a gas flow of 500 sccm through a quartz capillary with an inner diameter of 1 mm and a wall thickness of 0.25 mm. Two additional lateral gas flows, which amount to 1 slm, produce gas flow swirls on the substrate surface.
Plasma electrolytic oxidation is performed with an solution of distilled water with the addition of 1 g/l potassium hydroxide. |
Plasma Medium Procedure | During the substrate treatment with the DBD like He-plasma jet, the plasma jet nozzle is moved with a velocity of about 1 mm/s along the slit. The distance between the plasma jet nozzle and the glass plates surface amounts to 2 cm. |
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Contact Name | Gembus, Jan-Luca |
Plasma Target Properties | Aluminium alloy (AW-6061) with a dimension of 20 mm × 20 mm × 2 mm. |
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Plasma Diagnostic Properties | High-speed camera (Phantom VEO 440L 1MP; Vision Research): frame rate of 10 000 fps, exposure time of 99 μs and image resolution of 512 × 512 pixels.
he structure and composition of the treated substrates are characterised by surface scanning electron microscopy and energy dispersive x-ray spectroscopy using a scanning electron microscope (SEM)/energy dispersive x-ray spectroscopy (EDS) microscope (JSM6510, JEOL). |
Public Access Level | Public |
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Data and Resources
- Figure 3jpeg
SEM image of the surface of an aluminium substrate after preparation, namely...
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SEM images with different magnification of an anodised aluminium substrate (...
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